OEM and Replacement Heaters for Mass Spectrometers

Mini Clean Flow Heater
Mini Clean Flow Heater

MINI CLEAN FLOW HEATER

A very compact, fast responding electric heating element for liquids and gases for all clean, bio-med, laboratory, food, and pharmaceutical applications.




CAPILLARY SOURCE HEATER

Capillary Source Heater
Capillary Source Heater
The APCI (Atmospheric pressure chemical ionization) heater has a Resistance Temperature Detector (RTD) built into it.  The heater assembly has a .016” ID capillary tube in the center of the heater axis.  The maximum operating temperature is up to 400°C.  This assembly comes complete with the connector plug.

The APCI sample is typically dissolved in a solvent and pumped through a heated capillary.  Nitrogen gas is introduced, the gaseous solvent is heated up to 400°C and the sample is then ionized by corona discharge.

FLANGED GASLINE HEATER

Flanged Gasline Heater
Flanged Gasline Heater
This heater assembly is used in the electron ionization in gas chromatography and mass spectrometry to ionize and fragment analyte molecules before mass spectrometric analysis and detection.

A typical electron ionization source exposes the analyte, under vacuum to a stream of thermionic electrons produced from a resistively heated-gas weldment assembly. Gas heated up to 450°C. Built-in thermocouple for precise temperature control is incorporated in the gas body assembly.

CERAMIC HEATER

CeraWatt Ceramic Heater
CeraWatt Ceramic Heater
CeraWatt ceramic heating elements are composed of high temperature materials such as tungsten and alumina ceramic substrates. The metal heating resistance element is thick film technology. CeraWatt heaters provide excellent corrosion resistance, high operating temperature, long life, energy efficiency, uniform surface temperatures, and outstanding thermal conductivity.

Inline Gas Heaters: Precise Heat and Control without Contamination

Inline gas heaters are designed to heat clean gases or liquids without contaminating the stream. They provide exceptionally fast thermal response and high power densities in a compact package. The process fluid never comes in contact with the heating element directly, but instead, is shielded by a 316 stainless steel barrier. These heaters, often customized to suit a particular requirement, are available in a wide range of wattages and voltages. They are capable of high temperatures and heat and cool very rapidly due to their low mass.
Inline Electric Gas Heater for Clean Fluids
(BCE)

The heating elements are isolated electrically and physically from the process media, protecting them from contaminants and providing long life. The gas flow passes through the heater housing and over an enclosed heated body. The process media is never exposed to the resistive heating element. Inlet and outlet connections also come in a variety of sizes and types including NPT, SAE, BSP and VCR.

Applications:
  • Mass Spectrometers
  • Medical Devices
  • Pharma Analyzers
  • Lab Equipment
  • Semiconductor process

FAQ: Custom Heater Assemblies

Custom Heater Assemblies
Custom heater assembly that includes a sealed cartridge
heater, thermowell, and thermocouples (multiple).

What is a custom heater assembly?

In general terms, a custom heater assembly is a device that transforms electrical current to heat energy, is designed in a way that accommodates the needs of a unique heating requirement, and is used for the heating of gases, liquids, plastics, or metals.

What is a thermowell?

A thermowell is machined metallic tube used to house and protect sensors or heating elements. Thermowells not only protect heaters and sensors from erosive or corrosive media, they also allow for easy removal and replacement without exposing the process media.

What is a cartridge heater?

A cartridge heater is a cylindrically shaped electric heating element intended to be inserted in holes in metal platens or immersed in flowing media. The design incorporates a ceramic bobbin wound with nichrome resistance wire, carefully centered inside a metallic tube, and then backfilled with magnesium oxide (MgO), which provides electrical insulation. Cartridge heaters can be either swaged (compacted MgO) or un-swaged (loosely filled MgO). Swaging allows for maximum heat transfer to outside surfaces while keeping internal heater temperatures as low as possible, and preserving dielectric qualities.

What is a sealed cartridge heater?

A sealed cartridge heater incorporates all of the characteristics of a standard cartridge heater but is additionally sealed with BCE’s proprietary epoxy seal making it vacuum compatible. The seal additionally elongates heater life, especially in high humidity and moisture environments.

What electrical tests are performed on heaters?

Heaters undergo 3 main electrical tests: Resistance, MegOhm and Hipot.

A resistance test is performed using a fluke meter to ensure that the heater is manufactured within the correct tolerances of the electrical specifications. Heater leads are connected directly to the fluke meter leads to perform the test.

A MegOhm or Insulation Resistance test is performed using a megohmmeter. As its name implies it tests for any breakdown in a heater’s insulating material. The test is performed by supplying low to medium voltage to the insulating material for a small period of time.

A Hipot test is also used to assess the dielectric strength of the heater’s insulating material. In addition to performing a Dielectric Withstand Test like the Megohm, it can also perform a Dielectric Breakdown Test. This means that the heater insulating material is shocked at very high voltages until failure is achieved. This is more commonly performed on samples as it destroys the heater.

What is a thermocouple?

A thermocouple is a thermoelectric device that measures temperature. When the wire junction of its two dissimilar metals changes in temperature, a small voltage is created. The voltage is then used to calculate the temperature using the thermocouple’s reference table.

What is an RTD?

RTD stands for "resistance temperature detector". It is generally constructed of a fine and pure metallic wire wound around a ceramic or glass core. The relationship between wire resistance and temperature is used to sense the temperature of other devices.

Custom Heating Elements and Thermal System Design

The design and manufacture of custom heating elements and thermal systems are a specialty of BCE Inc. (Belilove Company-Engineers), a Hayward, California-based company that has served the aerospace, semiconductor, analytical and medical equipment industries for more than 25 years.

As both a manufacturer and integrator of components, BCE offers custom electrical heaters, sensors, and controls as discrete components, or as part of a larger, value added thermal system.

Visit https://bcemfg.com or call 510-274-199 for more information.

Vacuum Feedthrough FAQ

vacuum chamberWhat is a vacuum chamber?

It is an enclosure in which a low pressure or vacuum environment is created through the removal of air and gases.

What is a feedthrough?

Feedthroughs are electro-mechanical devices that provide leak-proof electrical and pressure connections into a vacuum chamber.

What is a hermetic seal on a feedthrough?

It provides an airtight seal against contaminants entering a vacuum chamber. Contaminants can include gases and fluids like moisture, humidity, and chemicals.

What processes are used to provide a hermetic seal?

Hermetic seals are generally processed in furnaces under regulated temperatures and pressures. They can be glass-to metal, ceramic-to-metal or epoxy based.

What metric is used to assess the hermeticity of a feedthrough?

Feedthroughs generally undergo helium leak checks to establish the helium leak rate, an indicator of the feedthroughs’ vacuum compatibility. Prior to a helium leak check, feedthroughs are visually inspected for cracks, damage and porosity in the seal.

What is the NASA ASTM E595 standard?

This standard pertains to epoxies that exhibit low Total Mass Loss and Collected Volatile Condensable Materials during Outgassing in a vacuum environment.

For information on vacuum feedthroughs, contact BCE by calling 510-274-1990 or by visiting the BCE website - https://bcemfg.com

New Electric Heater Design Maintains High Flow Rate of Cold Propellants and Optimizes Flow in Space Launches

BCE Hem Sealed Heater
Ideally a rocket engine would capitalize on internal heat dissipations to create a self-regulating thermal environment. However, in the majority of instances, maintaining a high flow rate of cold propellants can obstruct the flow path. Thus, it becomes essential to integrate resistive heaters inside the flow path’s valves and manifolds. Surface-mounted patch heaters are generally used for this application. These are polyimide/silicone sheathed resistive elements with one side adhered directly to the valves and manifolds. Although patch heaters may present a viable solution, the BCE HEM Sealed Heater™ outperforms as heat flows uniformly from inside the cartridge directly to the heated bodies.

This is because they are secured directly to components by the means of an integrated flange. In essence, the BCE HEM Sealed Heater™ incorporates both the cartridge heaters’ wire wound resistive element encased in a metal sheath and the vacuum compatibility of a feedthrough. Furthermore, the BCE proprietary epoxy seal allows the heater to pass strict electrical tests ensuring the purity of the dielectric materials and hence, preventing shorting.

SCOPE
  • Easy mounting of heaters into manifolds and valve bodies
  • Mounting to be compatible with standard hardware
  • 6 to 36V electrical specifications
  • Resistance tolerance to be +/-5%
  • < 1,500 VDC or greater on the Hi-pot test
  • < 4,000 Megohm at 500 to 1000 VDC on the Megohm test
  • < .010 sheath thickness
  • Sheath can be Inconel or 300 series stainless material
  • Sealing Epoxy to meet NASA ASTM E595 Low Outgassing Standard
  • Maximum operating temperature of heater <200°C

OUTCOME

The BCE HEM Sealed Heater™ proved to be the most optimal design for the heating of fast-flowing liquid propellants. The heater incorporated all engineering requirements and was mounted into the manifold through an integrated flange using custom hardware. In addition, the heater’s vacuum compatibility was ensured through BCE’s proprietary black epoxy meeting NASA ASTM E595. Furthermore, successful rocket launches into lower to high earth orbit validate that the BCE HEM Sealed Heater™ is rocket ready and capable of high vacuum applications. BCE, the ultimate partner for resistive vacuum applications.

Everything You Wanted to Know About Cartridge Heaters ...

Cartridge Heater
Cartridge Heater (Hotwatt Backer)
Reprinted with permission of Backer Hotwatt

WHAT ARE CARTRIDGE HEATERS?

Cartridge heaters originally consisted of a ceramic-supported heating wire inserted into round metal tube, making them look like cartridges (the likely source of their name). They provide localized heat to restricted working areas requiring close thermal control. Their power density is less than 60 W/in2 and they generate temperatures up to 1,200°F. They range in diameter from 1/8 to 2 in. and vary in length from less than an inch to over four feet. Although they are usually round, they can have square or rectangular cross sections. Standard cartridge heaters account for an estimated 20% of all electric heaters made.

Compacted cartridge heaters were developed about 60 years ago and feature inorganic powder tightly compacted onto the heater wire. This increases their power density to nearly 500 W/in2 and maximum temperatures approach 1,800°F. The need for higher quality tubing and precision-fired crushable ceramics makes compacted heaters cost 1.5 to 3 times the cost of a standard cartridge. They are available in diameters from 1/8 to 1 in. and lengths from 1 inch to over 3 feet.

HOW ARE CARTRIDGE HEATERS MADE?
Cartridge Heater
Cartridge Heater Internal View
For standard cartridge heaters, nickel / chromium heating coils are inserted in a ceramic tube inside a metal housing or sheath. Magnesium oxide filler is then vibrated into the hole to fill any voids. This increases heat transfer to the metal exterior. An end cap is welded on the bottom and insulated leads are installed at the opposite end. For swaged cartridge heaters, the nickel / chromium wire is wound around a ceramic core, placing the wire closer to the metal housing. Magnesium oxide is vibrated in and the heater swaged to a specific diameter. This compresses the MgO so it becomes a better conductor of heat while maintaining its dielectric properties. This improves heat transfer and allows for higher watt densities. Swaging also lets the heaters operate at higher temperatures and better withstand vibrations.

HOW CAN YOU GET THE MOST EFFICIENT HEAT TRANSFER AND LONGEST OPERATIONAL LIFE OUT OF A CARTRIDGE HEATER?
There are several steps users can take. On installation, for example, cartridge heaters should be installed in holes drilled and reamed to no more than 0.002 inches larger than needed. The heaters are routinely sized to never be 0.005 less than the nominal diameter and always at least .001 under the nominal diameter for a slide fit. These close fits ensure rapid heat transfer from the heater to the housing and helps keep the heater as cool as possible, which contributes to a long life. Heaters should not be cycled from low to high temperatures as it shortens their life considerably. Instead, designers should calculate the proper wattage for their applications. The best wattage results in a 50/50 off/on cycle. For temperatures over 750°F, off/on control can be replaced by input voltage regulation through variable transformers or proportioning controllers to minimize temperature fluctuations. If a heater is going to be turned off routinely, the air around it should be kept dry and no impurities (oil, gas,) should be in contact with the heater. That’s because the ceramic material used in cartridge heaters is hygroscopic. Every time power to the heater is switched off, it creates a vacuum inside the cooling housing which draws in air and any nearby impurities from the surrounding area. The moisture or impurities, once inside the housing, can cause a short circuit and result in heater failure.

If a thermostat is used to control the temperature, it should be no more than 0.5-in. from the heater. Mounting it any farther away could let the unit run hot and thereby shorten its life. Another cause of failures is too high a watt density. If the heater was incorrectly specified for an application and provides too much heat, the heater will not be able to dissipate the heat and will fail. Similarly, if the heater is designed for 120 V but is being powered by 240 V, the output wattage will be four times greater than it should be, which can, again, lead to failure.

WHAT OPTIONS ARE AVAILABLE ON CARTRIDGE HEATERS?
There are several options and variations available. Heaters may be three-phase or multiple wattage in a single unit. For instance, an application might need quick heat ups and then a standby circuit to maintain a relatively low temperature using different wattages based on changing thermal loads. Heaters can have wattage outputs that vary over their lengths in order to even out temperatures over a platen or a large surface. Heaters can also have built-in thermocouples, usually at the bottom of the heater and type J or K grounded or ungrounded. If a precision fit is needed, companies can supply centerless ground diameters. They can also supply certain heaters at higher voltages (300 to 600 V).
Heaters used in corrosive environments can be Teflon coated or electro-polished. Heaters that need hermetic sealing or will be used in a vacuum application can be ordered with ceramic-to-metal seals that withstand temperatures to 1,000°F.

CAN CARTRIDGE HEATERS BE USED IN LIQUIDS AS IMMERSION HEATERS?
Yes, when applied with a mount- ing fitting. Not all cartridge heaters made as immersion heaters are completely moisture sealed. The heater and bushing are submersible but the termination end is not necessarily sealed. If an application is in a high humidity area, however, the termination area should be sealed. Seals can be silicone rubber or Teflon which are good to 400°F, or epoxy potting which can handle temperatures to 265°F.

WHAT ARE SOME OF THE TERMINATION OPTIONS OFFERED ON CARTRIDGE HEATERS?
There are multiple options for cartridge heaters, almost too many to list. Standard options start with straight internally connected leads. External connections are optional on larger sizes, recommended when repairable leads are required. There are also post terminals available on cartridges 15⁄16-in. and larger. For applications with limited space, manufacturers can supply right-angle leads.

There are also several options for protecting leads. Fiberglass or silicone rubber sleeving, as well as ceramic bead insulation, protect against temperatures up to 1,000°F. Additional protection can be provided using flexible conduit or stainless steel braid.

Have a requirement for cartridge heaters? Call BCE now at 510-274-1990 or visit https://belilove.com